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Nitrazepam and 7-aminonitrazepam studied at the macroscopic and microscopic electrified liquid-liquid interface

dc.contributor.authorStelmaszczyk, Paweł
dc.contributor.authorKwaczyński, Karolina
dc.contributor.authorRudnicki, Konrad
dc.contributor.authorSkrzypek, Slawomira
dc.contributor.authorWietecha-Posłuszny, Renata
dc.contributor.authorPółtorak, Łukasz
dc.date.accessioned2023-08-01T17:17:33Z
dc.date.available2023-08-01T17:17:33Z
dc.date.issued2023
dc.identifier.citationStelmaszczyk, P., Kwaczyński, K., Rudnicki, K. et al. Nitrazepam and 7-aminonitrazepam studied at the macroscopic and microscopic electrified liquid-liquid interface. Microchim Acta 190, 182 (2023). https://doi.org/10.1007/s00604-023-05739-6pl_PL
dc.identifier.issn0026-3672
dc.identifier.urihttp://hdl.handle.net/11089/47741
dc.description.abstractTwo benzodiazepine type drugs, that is, nitrazepam and 7-aminonitrazepam, were studied at the electrified liquid-liquid interface (eLLI). Both drugs are illicit and act sedative in the human body and moreover are used as date rape drugs. Existence of the diazepine ring in the concerned chemicals structure and one additional amine group (for 7-aminonitrazepam) allows for the molecular charging below their pKa values, and hence, both drugs can cross the eLLI interface upon application of the appropriate value of the Galvani potential difference. Chosen molecules were studied at the macroscopic eLLI formed in the four electrode cell and microscopic eLLI formed within a microtip defined as the single pore having 25 μm in diameter. Microscopic eLLI was formed using only a few μL of the organic and the aqueous phase with the help of a 3D printed cell. Parameters such as limit of detection and voltammetric detection sensitivity are derived from the experimental data. Developed methodology was used to detect nitrazepam in pharmaceutical formulation and both drugs (nitrazepam and 7-aminonitrazepam) in spiked biological fluids (urine and blood).pl_PL
dc.description.sponsorshipR. Wietecha-Posłuszny and P. Stelmaszczyk are grateful for the financial support (National Science Centre, Grant no. UMO-2019/35/O/ST4/00978: application of developed extraction procedure, study the interfacial behavior of NIT and 7a-NIT), so is L. Poltorak (National Science Centre, Grant no. UMO-2018/31/D/ST4/03259: application of designed fused silica capillary and 3D printed cell for NIT and 7a-NIT detection).pl_PL
dc.language.isoenpl_PL
dc.publisherSpringer Naturepl_PL
dc.relation.ispartofseriesMicrochimica Acta;190:182
dc.rightsUznanie autorstwa 4.0 Międzynarodowe*
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/*
dc.subjectDate rape drugspl_PL
dc.subjectPsychoactive chemicalspl_PL
dc.subjectVoltammetrypl_PL
dc.subjectITIESpl_PL
dc.subjectElectrochemical sensorpl_PL
dc.titleNitrazepam and 7-aminonitrazepam studied at the macroscopic and microscopic electrified liquid-liquid interfacepl_PL
dc.typeArticlepl_PL
dc.page.number1-16pl_PL
dc.contributor.authorAffiliationLaboratory for Forensic Chemistry, Department of Analytical Chemistry, Faculty of Chemistry, Jagiellonian University, Gronostajowa 2, 30-387, Krakow, Polandpl_PL
dc.contributor.authorAffiliationElectrochemistry@Soft Interfaces Team, Department of Inorganic and Analytical Chemistry, Faculty of Chemistry, University of Lodz, Tamka 12, 91-403, Lodz, Polandpl_PL
dc.contributor.authorAffiliationElectrochemistry@Soft Interfaces Team, Department of Inorganic and Analytical Chemistry, Faculty of Chemistry, University of Lodz, Tamka 12, 91-403, Lodz, Polandpl_PL
dc.contributor.authorAffiliationElectrochemistry@Soft Interfaces Team, Department of Inorganic and Analytical Chemistry, Faculty of Chemistry, University of Lodz, Tamka 12, 91-403, Lodz, Polandpl_PL
dc.contributor.authorAffiliationLaboratory for Forensic Chemistry, Department of Analytical Chemistry, Faculty of Chemistry, Jagiellonian University, Gronostajowa 2, 30-387, Krakow, Polandpl_PL
dc.contributor.authorAffiliationElectrochemistry@Soft Interfaces Team, Department of Inorganic and Analytical Chemistry, Faculty of Chemistry, University of Lodz, Tamka 12, 91-403, Lodz, Polandpl_PL
dc.identifier.eissn1436-5073
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dc.contributor.authorEmaillukasz.poltorak@chemia.uni.lodz.ppl_PL
dc.contributor.authorEmailrenata.wietecha-posluszny@uj.edu.plpl_PL
dc.identifier.doi10.1007/s00604-023-05739-6
dc.disciplinenauki chemicznepl_PL


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Uznanie autorstwa 4.0 Międzynarodowe
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